Process for Preparing High Purity Sodium Tungstate Using High-Molybdenum Tungsten Ore
The present invention provides a method of treating high-molybdenum tungsten mineral or tungsten slime by means of three-ion column exchange molybdenum-eliminating technology so as to obtain Sodium Tungstate with high purity at low cost. The treating process includes grinding, alkali leaching, filtering and concentration to obtain sodium tungstate crystal; water dissolving, filtering and sulfurizing sodium tungstate; ion exchange to eliminate molybdenum; desulfurizing sodium tungstate liquid; ion exchange to eliminate impurity and desorbing tungsten with ammonia water and ammonium chloride solution to prepare ammonium tungstate solution; and evaporation to obtain ammonium para-tungstate crystal. The present invention has low cost.
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0.6um yellow tungsten oxide is a kind of tungsten oxide, with a positive yellow powder appearance, stable properties at normal temperature and apparent density of 0.6-1.0g/cm3.
Ammonium metatungstate(AMT) is an important intermediate compounds of tungsten hydrometallurgical process, appearance is white crystalline powder, solubility in water is the largest in the tungsten compounds which over 300g WO3/100ml H2O (in 25℃).
Sodium tungstate, a tungstate of sodium, is useful as a source of tungsten. It is prepared from tungsten ores used to manufacture tungsten by reducing it.
Purple Tungsten oxide is divided into WO2.72 (or W18O49). It is a kind of tungsten oxide. It is abbreviated as VTO. It is a purple finely grained crystalline powder, and its color usually appears purple or blue purple.